44355
Accession Number
9584
Title Of Article Chaper
An oxygen standard for the determination of oxygen in steel by 14 MeV neutron activation analysis
Title Of Journal Book
PREPRINTS; The 1968 International Conference, Modern Trends In Activation Analysis. National Bureau Of Standards
Pages
495-503
Literature Level
Analytic
Abstract
The standards and system described in this article have been used in the Seraing LD Steel Plant of S. A. Cockerill-Ougree- Providence (Liege, Belgium). The results obtained are sufficiently reproducible to warrant their metallurgical use. In addition, the rapidity of the method has been amply demonstrated; the preparation of the specimen from the frusto-conical-shaped bomb sample can be effected within 35 sec using an automatic lathe. Irradiation and counting time are 5 and 30 sec respectively; the results are computed automatically. The results of activation analysis agree satisfactorily with these obtained by various carburizing fusion methods. The standardization of the system is very simple. The preparation of the oxygen standard poses no special problems. Correction for differences in geometry and in neutron and gamma ray absorption is more complicated but must only be carried out once.
Keywords
metallurgy;steel;analysis
pub_id
44355