4418
Accession Number
4226
Author
Corbett, W.M.
Editor
Green, J.W.; Bemiller, J.N.
Title Of Article Chaper
6 Determination of the Alpha-cellulose Content of Cotton and Wood Cellulose
Title Of Journal Book
Methods in Carbohydrate Chemistry
Volume
3
Pages
27-28
Reference Bibliography
Includes bibliographical references
Publisher
Academic Press
Publisher City
New York;London
Language Of Text
English
Literature Type
Monograph
Literature Level
Analytic
Abstract
In order to purify cotton, carded cotton sliver is cut into short lengths, is extracted, preferably in a Soxhlet apparatus for 18 hr. with chloroform followed by 95% ethanol for a further 18 hr. It is vigorously boiled for 8 hr. in an atmosphere of nitrogen with 1% sodium hydroxide with a liquid ratio of 50 ml. per g., washed with water until free from alkali, and then washed sequentially with acetone, ethanol, and ether. The cellulose is then dried under reduced pressure at 20 degrees.
Keywords
cotton;cellulose;purification;test;chemical
pub_id
4418